                            INSTRUMENT CONTROL PARAMETERS:    GasMassa
                            ------------------------------------------

   D:\USERS\GIANLUCA SIMIONATO\METODI\METODO 1 NEW COL_SIMO.M
      Thu Nov 27 18:21:47 2025

Control Information
------- -----------

Sample Inlet      :  GC
Injection Source  :  GC ALS
Mass Spectrometer :  Enabled


 No Sample Prep method has been assigned to this method.

=============================================================================
                                 6850 GC METHOD
=============================================================================

OVEN
   Initial temp:  60 C (On)                Maximum temp:  325 C
   Initial time:  1.00 min                 Equilibration time:  0.10 min
   Ramps:
     #   Rate  Final temp  Final time
     1  15.00      290        3.00
     2    0 (Off)
   Post temp:  70 C
   Post time:  0.00 min
   Run time:  19.33 min

INLET (SPLIT/SPLITLESS)                 DETECTOR (NO DET)
   Mode:  Split                            Temperature:  280 C (On)
   Initial temp:  200 C (On)
   Pressure:  1.51 psi (On)
   Split ratio:  10:1
   Split flow:  10.0 mL/min
   Total flow:  14.6 mL/min
   Gas saver:  Off
   Gas type:  Helium

COLUMN                                  SIGNAL
   Capillary Column                        Save Data:  Off
   Model Number:  19091S-431E
   Description: HP-5MS  5% Phenyl Methyl
   Max temperature:  325 C
   Nominal length:  15.0 m
   Nominal diameter:  250.00 um
   Nominal film thickness:  0.25 um
   Mode:  constant flow
   Initial flow:  1.0 mL/min
   Nominal init pressure:  1.51 psi
   Average velocity:  52 cm/sec
   Source:  Inlet
   Outlet:  MSD
   Outlet pressure:  vacuum

VALVES                                  POST RUN
                                           Post Time: 0.00 min

TIME TABLE
   Time(min)      Parameter & Setpoint


INJECTOR
     Sample pre-washes:        3
     Sample pumps:             6
     Sample volume (uL): 1.000
     Syringe size (uL):     10.0
     Pre washes from bottle A:  3
     Pre washes from bottle B:  0
     Post washes from bottle A:  3
     Post washes from bottle B:  0
     Viscosity delay (seconds):  0
     Pre injection dwell (min):  0.00
     Post injection dwell (min):  0.00
     Sample skim depth (mm):   10.0(Off)
     NanoLiter Adapter Installed
     Solvent Wash Mode:  A, B
     Plunger Speed:  Fast
     Draw Speed (uL/min):  300
     Dispense Speed (uL/min):  6000
     Inject Speed (uL/min):  6000
     Solv Draw Speed (uL/min): 300
     Solv Dispense Speed (mL/min): 6000
     Multiple Injections: Off
     Solvent saver:  Off
     Normal Injection: On
     Air gap after Layer 1(uL): 0.200




 Column 1 Inventory Number :  
                                MS ACQUISITION PARAMETERS


General Information
------- -----------

Tune File                : atune.u
Acquistion Mode          : Scan


MS Information
-- -----------

Solvent Delay            : 3.00 min

EMV Mode                 : Relative
Relative Voltage         : 0
Resulting EM Voltage     : 1765

[Scan Parameters]

Low Mass                 : 50.0
High Mass                : 550.0
Threshold                : 150
Sample #                 : 2       A/D Samples    4
Plot 2 low mass          : 50.0
Plot 2 high mass         : 550.0

[MSZones]

MS Source                : 230 C   maximum 250 C
MS Quad                  : 150 C   maximum 200 C


                             END OF MS ACQUISITION PARAMETERS


                              TUNE PARAMETERS for SN: US11391702
                        -----------------------------

 Trace Ion Detection is OFF.

 EMISSION    :      34.610
 ENERGY      :      69.922
 REPELLER    :      22.416
 IONFOCUS    :      83.514
 ENTRANCE_LE :      25.500
 EMVOLTS     :    1764.706
                               Actual EMV  :    1764.71
                               GAIN FACTOR :       2.32
 AMUGAIN     :    2114.000
 AMUOFFSET   :     121.625
 FILAMENT    :       1.000
 DCPOLARITY  :       0.000
 ENTLENSOFFS :      18.824
 MASSGAIN    :    -557.000   
 MASSOFFSET  :     -38.000   

                           END OF TUNE PARAMETERS
                      ------------------------------------



                               END OF INSTRUMENT CONTROL PARAMETERS
                               ------------------------------------
